Adding Oil Fix S to Water-in-Silicone Sunscreen Formula to Prevent Separation

Asked by: prem.chunta On: June 11, 2020 Product Type: Cosmetics

Question

I have a starting sunscreen formula as follows:

Oil-Fix™ S (water-in-silicone, Silicone Gelling)

Ingredients:
Mirasil 318 6%
OMC (Same INCI) 8%
DHHB (Same INCI) 4%
BEMT (Same INCI) 3.5%
Octocrylene (340 nm Max length) 3%

Heat 70C

Mixing by Homogenizer
Titanium Dioxide 15 nm (Liquid) 3%
Titanium Dioxide 200 nm 2%
PMMA Booster 3%

Phenoxyethanol : DMDM 50:50 % 1%

Mixing by Homogenizer
Cyclopentasiloxane (Low Odor) 39%
BSG-350 (Cyclopentasiloxane and Dimethicone and Dimethicone/Vinyl Dimethicone Crosspolymer) 24%
Vitamin E 0.5%
Oil Fix S 1%
(Total 100%)

I would like to know at which step should I add Oil Fix S in the formula to prevent the separation of the yellow liquid, which is expected to be from Phase 1 (sunscreen agents)?

Answer

Recommended Steps for Incorporating Oil Fix S in Your Sunscreen Formula

Based on your sunscreen formula and the issue of yellow liquid separation, which is likely the oil-soluble sunscreen agents, the key is to ensure the Oil Fix S effectively stabilizes the phase containing these oils.

Oil Fix S is a gelling agent designed for silicones and oils, and it acts as a stabilizer for water-in-silicone emulsions by stabilizing the external silicone/oil phase. To prevent the separation of your sunscreen oils, Oil Fix S should be fully dispersed within the combined oil and silicone phase.

Here are the recommended steps for incorporating Oil Fix S into your formula:

  1. Combine all oil and silicone components: Mirasil 318, OMC, DHHB, BEMT, Octocrylene, Cyclopentasiloxane, BSG-350, and Vitamin E. Heat this mixture to 70°C.
  2. Add Oil Fix S to the heated oil/silicone mixture from step 1. Disperse thoroughly using a homogenizer to ensure Oil Fix S is fully incorporated and the oil/silicone phase is effectively gelled.
  3. Add the solid components: Titanium Dioxide 15 nm (Liquid), Titanium Dioxide 200 nm, PMMA Booster, and the preservative (Phenoxyethanol : DMDM 50:50 %).
  4. Homogenize the entire mixture until a uniform emulsion/dispersion is achieved.

By adding Oil Fix S to the combined oil and silicone phase early in the process, you help stabilize this external phase, which should prevent the separation of the oil-soluble sunscreen filters.