Achieving Clarity in PCMX and Pine Oil Formulation

Asked by: info.btc On: May 18, 2020 Product Type: Cosmetics

Question

Regarding a formulation using PCMX 4.8% + Pine Oil + Emulsifier:

When these ingredients are mixed, how can the resulting liquid be made clear?

Answer

Achieving Clarity with PCMX, Pine Oil, and a Solubilizer

When mixing oil-based ingredients like Pine Oil with water using a standard emulsifier, the result is typically a cloudy or milky emulsion. This is because the oil droplets are large enough to scatter light.

To achieve a clear solution, you need to use a specific type of emulsifier called a solubilizer. Solubilizers create much smaller dispersed particles (microemulsion), which do not scatter visible light, resulting in a clear appearance.

Additionally, the PCMX (Chloroxylenol) powder you are using needs to be dissolved in a suitable solvent before being incorporated into a water-based system. According to the product information, PCMX powder dissolves in organic solvents and glycols.

Here is a general approach to try and achieve a clear solution:

  1. Dissolve PCMX: Dissolve the PCMX powder in a suitable solvent such as Ethanol, Propylene Glycol, or another glycol. Ensure the PCMX is fully dissolved.
  2. Mix Pine Oil with Solubilizer: Combine the Pine Oil with a suitable solubilizer. The ratio of solubilizer to Pine Oil is crucial and needs to be determined through experimentation. A common starting point is 2-5 parts solubilizer to 1 part oil, but this can vary significantly depending on the specific ingredients.
  3. Combine Phases: Mix the dissolved PCMX/solvent solution with the Pine Oil/solubilizer mixture until well combined.
  4. Add to Water: Slowly add the combined oil/solvent/solubilizer phase to the water phase while stirring gently. Avoid vigorous mixing.

For clarity, you should use a solubilizer specifically designed for this purpose. Some suitable solubilizers to consider include:

  • Flora Solve™ Clear
  • Ultra Solve™
  • Eco Solve™
  • Free Solve™ (PEG-Free Solubilizer)
  • PPG-6-Decyltetradeceth-30

Important Considerations:

  • Ratio is Key: Finding the correct ratio of Pine Oil, Solubilizer, and the PCMX solvent relative to the water phase is critical for clarity. This requires careful testing.
  • Order of Addition: The typical order is to prepare the oil/solvent/solubilizer phase first and then slowly add it to the water.
  • Experimentation: You will need to perform small-scale tests to find the optimal ratios for your specific formulation to achieve a clear solution at 4.8% PCMX and your desired Pine Oil concentration.

Using a standard emulsifier will result in a cloudy product. Switching to a suitable solubilizer and finding the right ratios is the way to achieve clarity.