BB Cream Formulation Adjustment for High SPF, Water Resistance, and Stability
Question
I am developing a BB Cream formula and need advice on achieving the following properties and resolving issues:
Desired Properties:
- SPF 35 or higher (aiming for SPF 50+)
- Water resistance (suitable for heavy sweating)
- Good longevity/wear
- Improved coverage
- Preventing color dropping throughout the day
Proposed SPF 50+ Formula Ingredients & Percentages:
- BEMT: 3%
- Zinc Oxide 200nm EasyDisperse™: 10%
- Titanium Dioxide: 4%
- Tris-Biphenyl Triazine (Nano): 5%
- Water-Capsule™: Used as the emulsifier
- LipidSoft: 10%
- BB Micro Silk: Included for coverage and skin feel
- Silicone Gel Base (Ultra Clear) and Cyclomethicone: Considered for the oil phase
Specific Questions/Concerns:
- Is the proposed combination and percentage of sunscreens sufficient to achieve SPF 50+?
- Will 3% BEMT dissolve completely in the oil phase with only 10% LipidSoft (and no OMC)?
- Will the chosen sunscreens (BEMT, Zinc Oxide, Titanium Dioxide, Tris-Biphenyl Triazine) cause color dropping over time?
- How does the high oil phase percentage (37%) in this formula affect the long-term stability of the Water-in-Oil (W/O) emulsion using Water-Capsule™?
- Are the suggested mixing steps appropriate for this formula (heating oil phase to 70°C, mixing water phase until gel, adding oil to water gently)?
- How can I identify which ingredient in SPF Protect Ultra™ caused stinging when previously used?
- What is the current stock availability for Tris-Biphenyl Triazine (Nano)?
Answer
English Answer:
Regarding your request to adjust your BB cream formula for SPF 35/higher, water resistance, longevity, better coverage, and to prevent color dropping:
Increasing SPF:
- Your proposed SPF 50+ formula using BEMT 3%, Zinc Oxide 10%, Titanium Dioxide 4%, and Tris-Biphenyl Triazine (Nano) 5% can indeed achieve SPF 50 according to the staff's calculation.
- However, the staff noted that BEMT at 3% might not fully dissolve in the oil phase with only 10% LipidSoft. You may need to reduce the BEMT percentage or add more oil-soluble solvent (like OMC) to ensure complete dissolution during the heating step.
Coverage and Color Dropping:
- Adding BB Micro Silk is a good approach to improve coverage and skin feel (smoothness).
- The sunscreens in your proposed SPF 50+ formula (BEMT, Zinc Oxide, Titanium Dioxide, Tris-Biphenyl Triazine) are stable and are not known to cause color dropping due to degradation, unlike some other sunscreens (Avobenzone, OMC).
- The staff confirmed that Zinc Oxide 200nm EasyDisperse™ has very little whitening effect compared to Titanium Dioxide.
Silicone Gel Base and Cyclomethicone:
- You can include Silicone Gel Base (Ultra Clear) and Cyclomethicone in the oil phase if desired. However, remember they contribute to the total oil percentage.
High Oil Phase and Water-Capsule™ Stability:
- Your proposed formula has a high oil phase percentage (37%). While the staff has seen Water-Capsule™ work with higher oil percentages (up to 45% with Pro Polymer), 37% is above the typical recommendation (<= 25%) and may affect the long-term stability of the emulsion.
Water Resistance:
- Using Water-Capsule™ creates a Water-in-Oil (W/O) emulsion, which provides good water resistance suitable for handling heavy sweating, much better than an Oil-in-Water (O/W) formula.
Mixing Steps:
- The mixing steps provided by the staff are suitable for your proposed formula:
- Mix the oil phase ingredients and heat to 70°C to dissolve oil-soluble chemical sunscreens like BEMT.
- Mix the water phase ingredients until a gel forms.
- Add the oil phase to the water phase and mix gently until uniform.
- The mixing steps provided by the staff are suitable for your proposed formula:
SPF Protect Ultra™ Stinging:
- As the staff mentioned, the best way to identify which ingredient in SPF Protect Ultra™ caused the stinging is to test the individual components.
Tris-Biphenyl Triazine (Nano) Stock:
- The stock date mentioned in the conversation (April 1, 2016) is outdated. I cannot provide current stock availability information.
In summary, your SPF 50+ formula is feasible in terms of sun protection, provides good water resistance with Water-Capsule™, and the sunscreens used are stable against dropping. Pay attention to dissolving BEMT and note that the high oil phase might impact long-term stability. Adding BB Micro Silk will enhance coverage.
Related Products Mentioned
Light Cream Maker™
Silicone Gel (Ultra Clear, Super Silky)
Zinc Oxide 200nm EasyDisperse™
BB Micro Silk™
Beige Iron Oxides EasyMix™
Water-Capsule™ (Water-in-Oil Cream)