Formulating Cream/Lotion with High Oil Content (Hyaluron Liquid & Grapeseed Oil 50/50)

ถามโดย: sj_ying เมื่อ: December 03, 2013 ประเภทผลิตภัณฑ์: เครื่องสำอาง

คำถาม

I want to formulate a product by mixing `Double Hyaluron Liquid` and `Grapeseed Oil` at a 50/50 ratio. I initially thought of using `Polysorbate 20` as an emulsifier.

Could you please advise on the following:

1. Is `Polysorbate 20` suitable for creating a stable emulsion with a 50% oil phase? If not, which emulsifiers are suitable for this ratio?
2. What is the recommended usage percentage for suitable emulsifiers, and what are the mixing steps?
3. What kind of equipment is needed for mixing this formulation?
4. Do I need to include a preservative like `Phenoxyethanol` in this formula, and if so, at what percentage and when should it be added?

คำตอบ

Formulation Guidance: Double Hyaluron Liquid and Grapeseed Oil

Regarding your questions about mixing Double Hyaluron Liquid (water phase) and Grapeseed Oil (oil phase) at 50% each and using an emulsifier:

  1. Emulsifier Suitability:

    • You are correct that Polysorbate 20 (Tween 20) is generally used as a solubilizer for incorporating small amounts of oil (like essential oils or fragrances) into water, not for creating stable emulsions with high oil concentrations like 50%. Polysorbate 20 would not be suitable for emulsifying a 50% oil phase.
    • As suggested previously, Light Cream Maker™ or Satin Cream Maker™ are suitable emulsifiers for creating oil-in-water creams or lotions without needing heat.
    • Important Note on 50/50 Ratio: Both Light Cream Maker™ and Satin Cream Maker™ are designed to emulsify oil phases typically up to 20-25% of the total formula. Attempting to emulsify a 50% oil phase with these specific emulsifiers at their recommended usage rates (0.5-3%) is unlikely to result in a stable emulsion. The oil and water phases will likely separate over time.
    • To create a stable cream or lotion using Light Cream Maker™ or Satin Cream Maker™ with Double Hyaluron Liquid and Grapeseed Oil, it is highly recommended to adjust the ratio to have a lower oil percentage, ideally within the 20-25% range. For example, you could try a formula with 20-25% Grapeseed Oil, 74-79% Double Hyaluron Liquid (as the water phase), and 1% emulsifier (Light Cream Maker™ or Satin Cream Maker™).
    • Achieving a stable 50/50 oil-in-water emulsion typically requires a different type of emulsifier system specifically designed for high oil loads.
  2. Usage Percentage and Mixing Steps (using Light Cream Maker™ or Satin Cream Maker™ with a feasible oil %):

    • Usage Percentage: For Light Cream Maker™ or Satin Cream Maker™, a starting usage rate of 1-1.5% is generally recommended for emulsifying oil phases up to 20-25%. You might need to adjust this percentage slightly depending on the desired thickness and the exact oil content (within the 20-25% range).
    • Mixing Steps: These emulsifiers are cold-process, meaning they don't require heating the oil and water phases separately to high temperatures. A general method is:
      • Combine the water phase ingredients (e.g., Double Hyaluron Liquid and any other water-soluble ingredients). Stir until uniform.
      • Combine the oil phase ingredients (e.g., Grapeseed Oil and any other oil-soluble ingredients).
      • Add the emulsifier. For Light Cream Maker™, you can add it to either the oil or water phase. For Satin Cream Maker™, add it to the water phase and stir briefly before adding the oil phase.
      • Combine the oil phase with the water phase. Mix continuously using a stirrer until a cream or lotion texture forms. This usually happens within a few minutes.
  3. Mixing Equipment:

    • You can use a glass rod for small batches, but a low-speed mechanical stirrer or a cream mixer is more effective for achieving a smooth, uniform texture, especially for larger batches.
    • Important: Avoid high-speed mixing or spinning above 2500 rpm when using Light Cream Maker™ or Satin Cream Maker™, as this can damage the polymer structure and weaken the emulsion stability.
  4. Preservative (Phenoxyethanol):

    • Yes, it is essential to include a preservative like Phenoxyethanol (Extra Pure) in any cosmetic formulation containing water to prevent microbial growth and ensure product safety and shelf life.
    • The typical usage rate for Phenoxyethanol is 0.5-1.0%. For eye area products, the maximum recommended rate is 0.5%.
    • Mixing Step: Add Phenoxyethanol to the water phase during the mixing process. Ensure the temperature of the mixture is below 80°C when adding the preservative.

In summary, while mixing Double Hyaluron Liquid and Grapeseed Oil 50/50 is challenging with Light Cream Maker™ or Satin Cream Maker™, these emulsifiers are suitable for creating stable creams/lotions with a lower oil percentage (up to 20-25%). Always include a preservative like Phenoxyethanol in your water-based formulations.

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