Lotion Formulation: Mixing Steps, Solubility, and Texture

ถามโดย: junthima.phan เมื่อ: August 24, 2020 ประเภทผลิตภัณฑ์: เครื่องสำอาง

คำถาม

I need a lotion for skin nourishment and would like to inquire about the mixing steps before placing an order.

Ingredients:
Water Phase

  1. Purified Water 74.3%
  2. Safe-B3™ (Vitamin B3, Niacinamide) 5%
  3. CosmoWhite™ (1-Methylhydantoin-2-Imide) 1%
  4. Grape Seed Extract (Proanthocyanidins) 0.5%
  5. Panthenol (Vitamin B5) ExtraLite™ 2%
  6. DMAE (SkinTight MD™) Liquid 1%
  7. HydroAlgae™ 1%

Oil Phase

  1. Butylene Glycol 1%
  2. Soft Cream Maker™ 2%
  3. WhiteCumin™ (Tetrahydrodiferuloylmethane) 0.2%
  4. Gamma Oryzanol (Rice Bran Extract) 0.5%
  5. Vitamin E (Tocopheryl Acetate) 0.5%
  6. Argan Oil 5%
  7. Jojoba Oil 5%
  8. Mild Preserved Eco™ (Preservative-Free) 1%

Proposed Mixing Steps:

  1. Oil Phase: Combine 8+10+12+15 (no heat).
  2. Oil Phase: Combine 9+11+13+14, heat to dissolve, not exceeding 70°C.
  3. Wait for step (2) to cool below 40°C, then combine (1)+(2) and stir well.
  4. Water Phase: Combine all ingredients and stir well.
  5. Combine step (3) + (4) and blend well.

Questions:

  1. Are the mixing steps correct?
  2. Does the formula require adding Tween 20 for dissolving WhiteCumin™? (The recommendation says WhiteCumin™ dissolves in glycol or Tween 20 helps dissolve it).
  3. Is 1% Butylene Glycol sufficient? What percentage is needed for dissolution?
  4. What is the expected texture of this formula? I want a non-greasy nourishing lotion (for normal to dry skin) with a slightly fluid texture. Do I need to adjust the texture, and how?

Thank you.

คำตอบ

Lotion Formulation Review

Thank you for providing your lotion formula and mixing steps. Here is a review based on the ingredients and typical formulation practices:

Mixing Steps Review

Your proposed mixing steps have a few points that can be improved for better emulsification and stability, especially with Soft Cream Maker™. Soft Cream Maker™ requires heating in the oil phase and combining the hot oil phase with the hot water phase, followed by continuous stirring while cooling.

Here is a suggested revised mixing procedure:

  1. Prepare WhiteCumin™ Solution: In a small separate container, dissolve WhiteCumin™ (0.2%) in Butylene Glycol (1%). Stir until fully dissolved.
  2. Prepare Water Phase: Combine Purified Water (74.3%), Safe-B3™ (5%), CosmoWhite™ (1%), Grape Seed Extract (0.5%), Panthenol ExtraLite™ (2%), DMAE Liquid (1%), HydroAlgae™ (1%), and the WhiteCumin™/Butylene Glycol solution from step 1. Heat the Water Phase to 70°C.
  3. Prepare Oil Phase: Combine Soft Cream Maker™ (2%), Gamma Oryzanol (0.5%), Vitamin E (0.5%), Argan Oil (5%), and Jojoba Oil (5%). Heat the Oil Phase to 70°C, stirring until Soft Cream Maker™ and Gamma Oryzanol are melted/dissolved.
  4. Emulsification: Slowly add the hot Oil Phase (from step 3) to the hot Water Phase (from step 2) while stirring continuously with a mixer (e.g., stick blender or overhead stirrer). Maintain continuous stirring as the mixture cools down.
  5. Add Heat-Sensitive Ingredient: When the mixture has cooled below 40°C, add Mild Preserved Eco™ (1%).
  6. Final Mixing: Continue stirring until the lotion is fully cooled and uniform. The texture will continue to develop over the next 48 hours.

Specific Questions

  • Question 1: Mixing steps correctness. As reviewed above, the proposed steps need adjustment to properly incorporate Soft Cream Maker™ and ensure stable emulsification. The revised steps are provided above.
  • Question 2: Need for Tween 20. WhiteCumin™ can be dissolved in glycol or Polysorbate 20 (Tween 20). Since your formula already includes Butylene Glycol, which is a glycol, Polysorbate 20 is not strictly necessary for dissolving WhiteCumin™ if 1% Butylene Glycol is sufficient. However, adding a small amount of Polysorbate 20 could help ensure complete dissolution and dispersion of WhiteCumin™, although it would slightly alter the formula.
  • Question 3: Sufficiency of Butylene Glycol 1%. While Butylene Glycol can dissolve WhiteCumin™, 1% might be on the lower side to ensure complete dissolution of 0.2% WhiteCumin™, especially in a complex formula. To improve solubility assurance, you could consider increasing the Butylene Glycol percentage (e.g., to 2-5%) or using a small amount of Polysorbate 20 as mentioned in the previous point.
  • Question 4: Expected texture and adjustment. With 2% Soft Cream Maker™ and approximately 15.2% total oil phase, the resulting texture is likely to be a light lotion or even a serum-like consistency initially. Soft Cream Maker™ at 2% is below its recommended usage range (3-10%) for achieving significant viscosity. The texture will thicken over about 48 hours, but it may remain quite fluid. If you desire a slightly more viscous lotion texture, you could increase the Soft Cream Maker™ percentage (e.g., to 3-5%) or add a co-emulsifier/thickener like Cetyl Alcohol (1-3%). The oils used (Argan Oil, Jojoba Oil) are generally non-greasy and should contribute to a pleasant skin feel.

Hope this helps with your formulation!

ผลิตภัณฑ์ที่เกี่ยวข้องที่กล่าวถึง

Vitamin E (Tocopheryl Acetate)
Vitamin E (Tocopheryl Acetate)
เครื่องสำอาง
Safe-B3™ (Vitamin B3, Niacinamide)
Safe-B3™ (Vitamin B3, Niacinamide)
เครื่องสำอาง
Jojoba Oil (Golden - Deodorized)
Jojoba Oil (Golden - Deodorized)
เครื่องสำอาง
Argan Oil (Virgin - Deodorized)
Argan Oil (Virgin - Deodorized)
เครื่องสำอาง
Polysorbate 20 (Tween 20)
Polysorbate 20 (Tween 20)
เครื่องสำอาง
Pure-Oryzanol™ (gamma Oryzanol 97%, Rice Bran Extract)
Pure-Oryzanol™ (gamma Oryzanol 97%, Rice Bran Extract)
เครื่องสำอาง
Butylene Glycol
Butylene Glycol
เครื่องสำอาง
Panthenol (Vitamin B5) ExtraLite™
Panthenol (Vitamin B5) ExtraLite™
เครื่องสำอาง
DMAE (SkinTight MD™) Liquid
DMAE (SkinTight MD™) Liquid
เครื่องสำอาง
Soft Cream Maker™
Soft Cream Maker™
เครื่องสำอาง
WhiteCumin™ (Tetrahydrodiferuloylmethane)
WhiteCumin™ (Tetrahydrodiferuloylmethane)
เครื่องสำอาง
Mild Preserved Eco™ (Preservative-Free)
Mild Preserved Eco™ (Preservative-Free)
เครื่องสำอาง
Grape Seed Extract (Proanthocyanidins)
Grape Seed Extract (Proanthocyanidins)
เครื่องสำอาง
CosmoWhite™ (1-Methylhydantoin-2-Imide)
CosmoWhite™ (1-Methylhydantoin-2-Imide)
เครื่องสำอาง
HydroAlgae™
HydroAlgae™
เครื่องสำอาง