HPLC Analysis of Niacin (Nicotinic Acid) Impurities in Niacinamide

  • Product Code: 35536
Reverse-phase HPLC-UV method for quantification of nicotinic acid (niacin) as a process impurity in niacinamide (nicotinamide) powder.
฿3,990.00

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assignment คำแนะนำ

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description Sample Requirement

Solid (niacinamide powder) 0.1 grams

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ขั้นตอน ขั้นตอน ผลลัพธ์ที่คาดหวัง
1
Prepare phosphate...
check_circle_outline Clear buffer at pH 3.0.
2
Prepare mobile...
check_circle_outline Homogeneous mobile phase.
3
Sample: Weigh...
check_circle_outline Clear solution without particulates.
4
Standard: Dissolve...
check_circle_outline Clear standard solution.
5
Inject 20...
check_circle_outline Nicotinic acid Rt ~4.5 min, niacinamide ~7.5 min; impurity <=0.1% w/w relative to standard.

HPLC Analysis of Niacin (Nicotinic Acid) Impurities in Niacinamide
Reverse-phase HPLC-UV method for quantification of nicotinic acid (niacin) as a process impurity in niacinamide (nicotinamide) powder. Sample Requirement: Solid (niacinamide powder) 0.1 grams
Reverse-phase HPLC-UV method for quantification of nicotinic acid (niacin) as a process impurity in niacinamide (nicotinamide) powder. Sample Requirement: Solid (niacinamide powder) 0.1 grams
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Service Steps
Step Procedure Expected Result
1 Prepare phosphate... Clear buffer at pH 3.0.
2 Prepare mobile... Homogeneous mobile phase.
3 Sample: Weigh... Clear solution without particulates.
4 Standard: Dissolve... Clear standard solution.
5 Inject 20... Nicotinic acid Rt ~4.5 min, niacinamide ~7.5 min; impurity <=0.1% w/w relative to standard.